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[DOI] [PubMed] [Google Scholar] 29.Ruggeri R.M., Giovinazzo S., Barbalace M.C., Cristani M., Alibrandi A., Vicchio T.M., Giuffrida G., Aguennouz M.H., Malaguti M., Angeloni C., et al

Both the organic and aqueous layers were separated and acidified the aqueous layer with aq.HCl solution