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Because research-market material is sold outside any approved supply chain, its identity and purity are unverified: published trial data describe a characterized study drug, not the contents of an arbitrary vial, so identity confirmation (for example by mass spectrometry and HPLC) and a batch certificate of analysis are the minimum a rigorous research setting should require

Urine was collected as a spot baseline sample and a sample after 24-hour challenge

The regulatory environment continues to evolve, and researchers should stay informed about current restrictions